Citation: LIU Zong-Guang, QU Shu-Xin, ZHAO Jun-Sheng, LIU Yu, WENG Jie. Influence of Dopamine on Physicochemical Properties of Calcium Phosphate Cement[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(3): 507-515. doi: 10.3969/j.issn.1001-4861.2013.00.088
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The aim of this study is to investigate effects of dopamine (DA) on physiochemical properties of calcium phosphate cement (CPC) and in vitro degradation of DA from CPC. DA was dissolved in Tris (Hydroxymethyl) aminomethane-hydrochloric acid buffer solution and mixed the solution with CPC powders after oxidized for 2 d in air. Orthogonal test was used to optimize the preparation of CPC with respect to the DA concentration, ratio of liquid to solid and pH values. Compressive tests, Gilmore needle tests, X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) were used to characterize the physiochemical properties of CPC. Scanning electron microscope (SEM) and UV-Vis spectrophotometry were used to observe the micro-morphology of CPC and in vitro degradation of DA from CPC, respectively. Compressive test and orthogonal analysis indicated that the optimal combination CPC was DA concentration 40 mg·mL-1, ratio of liquid to solid 0.3 mL·g-1 and pH value 8.5, which had the highest compressive strength with significant difference (p<0.01) compared with that of CPC-Blank. Setting time of the optimal combination CPC decreased slight but no significant difference compared to that of CPC-Blank, which could satisfied with the clinical demands. XRD and FTIR demonstrated that the addition of DA promoted the conversion of dicalcium phosphate dehydrate (DCPD). SEM found that there were more platy structure, lots of nubbly crystals and less porosity in optimal combination CPC compared with CPC-Blank. Cumulative release of DA from CPC was 29.7% and the pH values of immersion solution were safe for human body during in vitro degradation.
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-
[1]
[1] Espanol M, Perez R A, Montufar E B, et al. Acta. Biomater., 2009,5:2752-2762
-
[2]
[2] Nezafati N, Moztarzadeh F, Hesaraki S, et al. Ceram. Int., 2011,37:927-934
-
[3]
[3] WEI Jie(魏杰), LIU Chang-Sheng(刘昌胜), HONG Hua(洪 华), et al. Chinese J. Inorg. Chem.(Wuji Huaxue Xuebao), 2006,22(4):765-770
-
[4]
[4] ZHAO Ping(赵萍), SUN Kang-Ning(孙康宁), ZHU Guang-Nan(朱广楠). J. Chin. Ceram. Soc.(Guisuanyan Xuebao), 2005,33(1):32-35,46
-
[5]
[5] MA Li-Xin(马立新), YANG Nan-Ru(杨南如), CHEN Jian-Hua(陈建华). J. Ceram.(Taoci Xuebao), 2003,24(2):98-102
-
[6]
[6] HU Yun-Sheng(胡运生), FAN Qing-Yu(范清宇), MA Bao-An(马保安), et al. J. Funct. Mater.(Gongneng Cailiao), 2006, 4(37):607-610
-
[7]
[7] Chewa K K, Lowa K L, Zeina S H S, et al. J. Mech. Behav. Biomed., 2011,4(3):331-339
-
[8]
[8] ZHAO Xiao-Yun(赵晓云), GUO Da-Gang(郭大刚), HAN Yong(憨勇), et al. Chinese J. Inorg. Chem.(Wuji Huaxue Xuebao), 2005,20(5):1167-1173
-
[9]
[9] Ginebra M P, Rilliard A, Fernández E, et al. J. Biomed. Mater. Res., 2001,57(1):113-118
-
[10]
[10] Lin J, Zhang S, Chen T, et al. J. Biomed. Mater. Res., 2006, 76(2):432-439
-
[11]
[11] ZHANG Tao(张涛), GAO Jie-Wei(高杰维), QU Shu-Xin(屈 树新), et al. Chinese J. Inorg. Chem.(Wuji Huaxue Xuebao), 2010,26(6):957-962
-
[12]
[12] SUN Pei-Yu(孙培育), TIAN Li-Ying(田立颖), ZHEN Zhen (郑震), et al. Acta Polym. Sin.(Gaofenzi Xuebao), 2009,8: 803-808
-
[13]
[13] XU You-Yi(徐又一), JIANG Jin-Hong(蒋金泓), ZHU Li-Ping(朱利平), et al. Membr. Sci. Technol.(Mo Kexue Yu Jishu), 2011,31(3):32-38
-
[14]
[14] Yin M, Yuan Y, Liu C S, et al. Biomaterials, 2009,30:2764-2773
-
[15]
[15] Waite J H. Nat. Mater., 2008,7:8-9
-
[16]
[16] Lee H, Dellatore S M, Miller W M, et al. Science, 2007, 318:426-430
-
[17]
[17] Ku S H, Ryu J, Hong S K, et al. Biomaterials, 2010,31: 2535-2541
-
[18]
[18] Fei B, Qian B, Yang Z, et al. Carbon, 2008,46:1795-1797
-
[19]
[19] Kang S M, You I, Cho W K, et al. Angew. Chem. Int. Edit., 2010,49:9401-9404
-
[20]
[20] XIE Bin(谢槟), LI Gui-Cai(李贵才), DAI Lu(代璐), et al. Chem. J. Chinese Universities(Gaodeng Xuexiao Huaxue Xuebao), 2012,33(1):90-95
-
[21]
[21] JIANG Xiao-Xin(姜晓鑫), QU Shu-Xin(屈树新), LIN Sun-Zhong(林孙忠), et al. J. Inorg. Mater.(Wuji Cailiao Xuebao), 2011,26(1):29-37
-
[22]
[22] Oreffo R O C, Driessens F C M, Planell J A, et al. Biomaterials, 1998,19(20):1845-1854
-
[23]
[23] Herlinger E, Jameson R F, Linert W. J. Chem. Soc. Pakistan., 1995,2:259-263
-
[24]
[24] SHEN Wei(沈卫), GU Yan-Fang(顾燕芳), LIU Chang-Sheng (刘昌胜). J. East. Chin. Univ. Sci. Technol.(Huadong Ligong Daxue Xuebao), 1997,23(5):580-584
-
[25]
[25] GAO Cheng-Ying(郜成莹), YE Jian-Dong(叶建东). Mater. Rev.(Cailiao Daobao), 2008,22(3):151-154
-
[26]
[26] 国家药典委员会. Chinese Pharmacopoeia: Vol.2(中华人 民共和国药典:第2部). Beijing: Medicine Science and Technology Press of China, 2010.
-
[27]
[27] ZHANG Rong-Fa(张荣发), LIAO Ai-Di(廖爱娣), ZHANG Shu-Fang(张淑芳), et al. Chin. J. Nonferrous. Metal (Zhongguo Youse Jinshu Xuebao), 2011,21(4):927-931
-
[28]
[28] Ginebra M P, Fernández E, Boltong M G, et al. Clin. Mater., 1994,17(2):99-104
-
[29]
[29] LI Mao-Hong(李茂红), QU Shu-Xin(屈树新), YAO Ning(姚 宁), et al. J. Inorg. Mater.(Wuji Cailiao Xuebao), 2010,25 (5):507-511
-
[30]
[30] Kim S, Park C B. Biomaterials, 2010,31:6628-6634
-
[31]
[31] Lee M, Ku S H, Ryu J, et al. J. Mater. Chem., 2010,20: 8848-8853
-
[32]
[32] QU Shu-Xin(屈树新). Thesis for the Doctorate of Sichuan University(四川大学博士论文). 2002.
-
[33]
[33] CHEN Hou(陈厚). Analysis Test and Research Methods of Polymer Materials. 1st Ed(高分子材料分析测试与研究方 法.1版). Beijing: Chemical Industry Press, 2011.
-
[34]
[34] WAN Peng(万鹏), TONG Hua(童华), ZHU Ming-Yan(朱明 彦), et al. Proceedings of Second Chinese Biological Compound Material Conference(第二届中国生物复台村料 研讨会论文集). Tianjin:[s.n.], 2005:202-207
-
[35]
[35] Bohner M. Injury, 2000,31:37-47
-
[36]
[36] GUO Yue-Hua(郭悦华). Thesis for the Master of Southwest Jiaotong University(西南交通大学硕士论文). 2008.
-
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