Citation: YUAN Wei, LIU Fang, ZHANG Zhao. Preparation and Characterization of Mesoporous Nickel Oxide Templated by Different Mixed Surfactants[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(4): 803-809. doi: 10.3969/j.issn.1001-4861.2013.00.052
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Mesoporous nickel oxide was prepared by hydrothermal method using Ni(NO3)2·6H2O as the nickel source, urea as the precipitant and mixed surfactant SDS/P123, CTAB/P123, CTBA/SDS as the template, at a low consumption of total surfactant. The precursor and final products were characterized by TG-DSC, FTIR, XRD, N2 adsorption-desorption, SEM and TEM. Electrochemical performances were examined by cyclic voltammetry, constant current charge-discharge and electrical impedance spectroscopy. The results show that NiO templated by mixed surfactant SDS/P123 has the highest specific surface area, pore volume and capacitance of 209 m2·g-1, 0.407 cm3·g-1 and 265 F·g-1, respectively, when the mass ratio of mSDS:mP123=2:1.
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