Preparation of Benzamide by Hydration of Benzonitrile with Palladium Acetate and Phenylarsonic Acid as Synergistic Catalyst
- Corresponding author: HU Chang-Wen, cwhu@bit.edu.cn
Citation: WANG Tao, LIN Zheng-Guo, HU Chang-Wen. Preparation of Benzamide by Hydration of Benzonitrile with Palladium Acetate and Phenylarsonic Acid as Synergistic Catalyst[J]. Chinese Journal of Inorganic Chemistry, ;2019, 35(9): 1619-1622. doi: 10.11862/CJIC.2019.181
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Reaction conditions: Pd(OAc)2 (15 μmol, 3.36 mg), PhAsO3H2 (10 μmol, 2.02 mg), benzonitrile (1 mL), water (0.5 mmol, 9 μL), 90 ℃ and 0.5 h
Inset: photographs of (a) reaction at 90 ℃ for 0.5 h, (b) cooling from 90 to 25 ℃