Preparation and Adsorption Properties of Amino Modified Magnetic Mesoporous Microsphere Fe3O4@SiO2@mSiO2
- Corresponding author: XUE Juan-Qin, huagong1985@163.com MA Jing, majing@xauat.edu.cn
Citation: XUE Juan-Qin, XU Shang-Yuan, ZHU Qian-Wen, QIANG Liang-Sheng, MA Jing. Preparation and Adsorption Properties of Amino Modified Magnetic Mesoporous Microsphere Fe3O4@SiO2@mSiO2[J]. Chinese Journal of Inorganic Chemistry, ;2016, 32(9): 1503-1511. doi: 10.11862/CJIC.2016.215
LI Guang-Lu, HE Tao, LI Xue-Mei. J. Prog. Chem., 2011, 23(6):1081-1089
Laurent S, Forge D, Port M, et al. Chem. Rev., 2008, 108: 2064-2110
doi: 10.1021/cr068445e
WANG Miao-Miao, LI Qun-Yan, WEI Qi, et al. Chem. J. Chinese Universities, 2013, 34(2):299-305
XIONG Shan, JIANG Xiang-Ping, LI Ju-Mei, et al. J. Chin. Ceram. Soc., 2015, 43 (7):946-951
LIU Yun-Fang, REN Sen, WU Ri-Liang, et al. Chinese J. Inorg. Chem., 2015, 31(12):2373-2378
Park M, Seo S, Lee I S, et al. Chem. Commun., 2010, 46: 4478-4480
doi: 10.1039/c002905j
Wu P G, Zhu J H, Xu Z H. Adv. Funct. Mater., 2004, 14(4): 345-351
doi: 10.1002/(ISSN)1616-3028
Liu Y, Fu R, Sun Y, et al. Appl. Surf. Sci., 2016, 369:267-276
doi: 10.1016/j.apsusc.2016.02.043
Morel A L, Nikitenko S I, Gionnet K, et al. ACS Nano, 2008, 2(5):847-856
doi: 10.1021/nn800091q
Stjerndahl M, Andersson M, Hall H E, et al. Langmuir, 2008, 24(7):3532-3536
doi: 10.1021/la7035604
Zhao W R, Gu J L, Zhang L X, et al. J. Am. Chem. Soc., 2005, 127(25):8916-8917
doi: 10.1021/ja051113r
Fu R, Jin X M, Liang J L, et al. J. Mater. Chem., 2011, 21: 15352-15356
doi: 10.1039/c1jm11883h
WANG Rong, HAN Hai-Zhou, ZHENG Xing-Wang, et al. Acta Chim. Sinica, 2010, 68(17):1726-1734
SHEN Bin, WANG Yong-An, WANG Zhi-Fei, et al. Acta Phys.-Chim. Sin., 2010, 26(7):1860-1866
Bao S, Tang L, Li K, et al. J. Colloid Interface Sci., 2016, 462:235-242
doi: 10.1016/j.jcis.2015.10.011
Yang J, Shen D, Wei Y, et al. Nano Res., 2015, 8(8):2503-2514
doi: 10.1007/s12274-015-0758-2
Tan H, Xue J M, Shuter B, et al. Adv. Funct. Mater., 2010, 20:722-731
doi: 10.1002/adfm.v20:5
Li Y, Sun J, Zhang L, et al. Appl. Surf. Sci., 2012, 258: 3333-3339
doi: 10.1016/j.apsusc.2011.06.159
Panella B, Vargas A, Baiker A. J. Catal., 2009, 261:88-93
doi: 10.1016/j.jcat.2008.11.002
Baby T T, Ramaprabhu S. Talanta, 2010, 80:2016-2022
doi: 10.1016/j.talanta.2009.11.010
Gai S, Yang P, Li C, et al. Adv. Funct. Mater., 2010, 20:1-7
XUE Hong-Tao, SHEN Shui-Fa, PAN Hai -Bo, et al. J. Inorg. Mater., 2009, 24(3):577-580
Nagao D, Satoh T, Konno M. J. Colloid Interface Sci., 2000, 232(1):102-110
doi: 10.1006/jcis.2000.7195
Weng C H, Wang J H, Huang C P. Water Sci. Technol., 1997, 35:55-62
Ho Y S, McKay G. Proc. Biochem., 1999, 34(5):451-465s
doi: 10.1016/S0032-9592(98)00112-5
Endong YANG , Haoze TIAN , Ke ZHANG , Yongbing LOU . Efficient oxygen evolution reaction of CuCo2O4/NiFe-layered bimetallic hydroxide core-shell nanoflower sphere arrays. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 930-940. doi: 10.11862/CJIC.20230369
Youlin SI , Shuquan SUN , Junsong YANG , Zijun BIE , Yan CHEN , Li LUO . Synthesis and adsorption properties of Zn(Ⅱ) metal-organic framework based on 3, 3', 5, 5'-tetraimidazolyl biphenyl ligands. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1755-1762. doi: 10.11862/CJIC.20240061
Xiaosong PU , Hangkai WU , Taohong LI , Huijuan LI , Shouqing LIU , Yuanbo HUANG , Xuemei LI . Adsorption performance and removal mechanism of Cd(Ⅱ) in water by magnesium modified carbon foam. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1537-1548. doi: 10.11862/CJIC.20240030
Jingke LIU , Jia CHEN , Yingchao HAN . Nano hydroxyapatite stable suspension system: Preparation and cobalt adsorption performance. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1763-1774. doi: 10.11862/CJIC.20240060
Xiaoning TANG , Shu XIA , Jie LEI , Xingfu YANG , Qiuyang LUO , Junnan LIU , An XUE . Fluorine-doped MnO2 with oxygen vacancy for stabilizing Zn-ion batteries. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1671-1678. doi: 10.11862/CJIC.20240149
Peng XU , Shasha WANG , Nannan CHEN , Ao WANG , Dongmei YU . Preparation of three-layer magnetic composite Fe3O4@polyacrylic acid@ZiF-8 for efficient removal of malachite green in water. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 544-554. doi: 10.11862/CJIC.20230239
Chuanming GUO , Kaiyang ZHANG , Yun WU , Rui YAO , Qiang ZHAO , Jinping LI , Guang LIU . Performance of MnO2-0.39IrOx composite oxides for water oxidation reaction in acidic media. Chinese Journal of Inorganic Chemistry, 2024, 40(6): 1135-1142. doi: 10.11862/CJIC.20230459
Siyu HOU , Weiyao LI , Jiadong LIU , Fei WANG , Wensi LIU , Jing YANG , Ying ZHANG . Preparation and catalytic performance of magnetic nano iron oxide by oxidation co-precipitation method. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1577-1582. doi: 10.11862/CJIC.20230469
Yuanpei ZHANG , Jiahong WANG , Jinming HUANG , Zhi HU . Preparation of magnetic mesoporous carbon loaded nano zero-valent iron for removal of Cr(Ⅲ) organic complexes from high-salt wastewater. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1731-1742. doi: 10.11862/CJIC.20240077
Qi Li , Pingan Li , Zetong Liu , Jiahui Zhang , Hao Zhang , Weilai Yu , Xianluo Hu . Fabricating Micro/Nanostructured Separators and Electrode Materials by Coaxial Electrospinning for Lithium-Ion Batteries: From Fundamentals to Applications. Acta Physico-Chimica Sinica, 2024, 40(10): 2311030-. doi: 10.3866/PKU.WHXB202311030
Yonghui ZHOU , Rujun HUANG , Dongchao YAO , Aiwei ZHANG , Yuhang SUN , Zhujun CHEN , Baisong ZHU , Youxuan ZHENG . Synthesis and photoelectric properties of fluorescence materials with electron donor-acceptor structures based on quinoxaline and pyridinopyrazine, carbazole, and diphenylamine derivatives. Chinese Journal of Inorganic Chemistry, 2024, 40(4): 701-712. doi: 10.11862/CJIC.20230373
Xiutao Xu , Chunfeng Shao , Jinfeng Zhang , Zhongliao Wang , Kai Dai . Rational Design of S-Scheme CeO2/Bi2MoO6 Microsphere Heterojunction for Efficient Photocatalytic CO2 Reduction. Acta Physico-Chimica Sinica, 2024, 40(10): 2309031-. doi: 10.3866/PKU.WHXB202309031
Guimin ZHANG , Wenjuan MA , Wenqiang DING , Zhengyi FU . Synthesis and catalytic properties of hollow AgPd bimetallic nanospheres. Chinese Journal of Inorganic Chemistry, 2024, 40(5): 963-971. doi: 10.11862/CJIC.20230293
Zhaoyang WANG , Chun YANG , Yaoyao Song , Na HAN , Xiaomeng LIU , Qinglun WANG . Lanthanide(Ⅲ) complexes derived from 4′-(2-pyridyl)-2, 2′∶6′, 2″-terpyridine: Crystal structures, fluorescent and magnetic properties. Chinese Journal of Inorganic Chemistry, 2024, 40(8): 1442-1451. doi: 10.11862/CJIC.20240114
Liang MA , Honghua ZHANG , Weilu ZHENG , Aoqi YOU , Zhiyong OUYANG , Junjiang CAO . Construction of highly ordered ZIF-8/Au nanocomposite structure arrays and application of surface-enhanced Raman spectroscopy. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1743-1754. doi: 10.11862/CJIC.20240075
Jie ZHAO , Sen LIU , Qikang YIN , Xiaoqing LU , Zhaojie WANG . Theoretical calculation of selective adsorption and separation of CO2 by alkali metal modified naphthalene/naphthalenediyne. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 515-522. doi: 10.11862/CJIC.20230385
Jiahong ZHENG , Jiajun SHEN , Xin BAI . Preparation and electrochemical properties of nickel foam loaded NiMoO4/NiMoS4 composites. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 581-590. doi: 10.11862/CJIC.20230253
Limei CHEN , Mengfei ZHAO , Lin CHEN , Ding LI , Wei LI , Weiye HAN , Hongbin WANG . Preparation and performance of paraffin/alkali modified diatomite/expanded graphite composite phase change thermal storage material. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 533-543. doi: 10.11862/CJIC.20230312
Jingjing QING , Fan HE , Zhihui LIU , Shuaipeng HOU , Ya LIU , Yifan JIANG , Mengting TAN , Lifang HE , Fuxing ZHANG , Xiaoming ZHU . Synthesis, structure, and anticancer activity of two complexes of dimethylglyoxime organotin. Chinese Journal of Inorganic Chemistry, 2024, 40(7): 1301-1308. doi: 10.11862/CJIC.20240003
Xiaoling LUO , Pintian ZOU , Xiaoyan WANG , Zheng LIU , Xiangfei KONG , Qun TANG , Sheng WANG . Synthesis, crystal structures, and properties of lanthanide metal-organic frameworks based on 2, 5-dibromoterephthalic acid ligand. Chinese Journal of Inorganic Chemistry, 2024, 40(6): 1143-1150. doi: 10.11862/CJIC.20230271
N2 adsorption-desorption isotherm of Fe3O4@SiO2
(a) Fe3O4, (b) Fe3O4@SiO2, (c) Fe3O4@SiO2@mSiO2(0.35), (d) Fe3O4@SiO2@mSiO2(0.45), (e) Fe3O4@SiO2@mSiO2(0.67), (f) Fe3O4@SiO2@mSiO2-NH2
SEM images: (a) Fe3O4, (b) Fe3O4@SiO2, (c) Fe3O4@SiO2@mSiO2(0.45); TEM images: (d) Fe3O4, (e) Fe3O4@SiO2@mSiO2(0.35), (f) Fe3O4@SiO2@mSiO2(0.45), (g) Fe3O4@SiO2@m SiO2(0.67), (h) Fe3O4@SiO2@mSiO2-NH2; Inset in (h): enlarged view of pore structure