Citation: WU Xiao-Dong, SHAO Gao-Feng, CUI Sheng, WANG Ling, SHEN Xiao-Dong. Preparation and Characterization of SiO2/Carbon Foam and SiC/Carbon Foam Composites[J]. Chinese Journal of Inorganic Chemistry, ;2015, (6): 1252-1260. doi: 10.11862/CJIC.2015.161
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The synthesis and characterization of carbon foam supported silica aerogel (SiO2/Carbon foam) and silicon carbide composite (SiC/Carbon foam) are presented in this study. The phase composition, microstructure, thermal and mechanical properties are investigated by XRD, SEM, LFA Laser Flashmeasurements, and Universal Material Testing.The resulting SiO2/Carbon foam composite shows a higher compressive strength (14.95 MPa) and a smaller thermal conductivity (0.44 W·m-1·K-1) at room temperature, in comparison with the pristine carbon foam. The SiC/Carbon foam composite maintains a compressive strength of 14.66 MPa, and possesses a low high-temperature thermal conductivity (2.18 W·m-1·K-1 at 1200 ℃). Mass loss does not begin until 610 ℃ for the SiC/Carbon foam composite, and complete carbon combustion does not occur until 844 ℃, indicating a much better thermal stability than the pristine carbon foam in oxidizing atmosphere.
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