Citation: LIU Xi-Hui, ZHUO Xin, LIU Chao, LIU Tai-Zhu. Synthesis and Crystal Structure of Two 3D Networks Ni(Ⅱ)/Co(Ⅱ) Coordination Complexes Based on Bipyridine and Methanoic acid[J]. Chinese Journal of Inorganic Chemistry, ;2014, 30(5): 1128-1134. doi: 10.11862/CJIC.2014.142
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Two transition metal complexes, [M(bipy)(Metha)2]n·nH2O (M=Ni, 1; Co, 2; bipy=4,4'-bipyridine, Metha=methanoic acid), have been synthesized by hydrothermal synthesis and characterized by elemental analyses, IR spectroscopy, and X-ray single-crystal diffraction etc. The single crystal structures show the two complexes belong to monoclinic system, C2/c space group. Complexes 1 and 2 have similar 3Dnetwork structures. Metha have two kinds of different types with M2+ ion, one kind is the two oxygen atoms of the Metha as bridging ligand atoms, connected by chain with bipy, another is the carboxyl oxygen of the Metha with only one oxygen atom with another M2+ ion.
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