Citation: MA Tao, LIU Tao-Tao, YANG Yan-Yan, HUANG Yuan-Biao*, CAO Rong*. In Situ Preparation of Palladium Nanoparticles Supported on ZIF-8 for Suzuki-Miyaura Reaction[J]. Chinese Journal of Inorganic Chemistry, ;2014, 30(1): 127-133. doi: 10.11862/CJIC.2014.079 shu

In Situ Preparation of Palladium Nanoparticles Supported on ZIF-8 for Suzuki-Miyaura Reaction

MA Tao ^1,2 ,
LIU Tao-Tao ^1,2 ,
YANG Yan-Yan ^1,2 ,
HUANG Yuan-Biao* ² ,
CAO Rong* ²

1.
1 College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou 350002, China;

Received Date: 25 September 2013
Available Online: 29 November 2013
Fund Project:

Highly dispersed palladium nanoparticles (Pd NPs) supported on zeolitic imidazolate frameworks (ZIFs) ZIF-8 (Pd/ZIF-8) have been prepared in situ via mechanochemical method. The Pd/ZIF-8 frameworks were characterized by XRD, N₂ adsorption, TEM, ICP-AES and XPS. The results show that bulk production of highly dispersed palladium nanoparticles can be achieved by mechanochemical method. Moreover, the obtained Pd/ZIF-8 exhibits high activity for Suzuki-Miyaura cross-coupling reaction and can be easily recovered and reused.
- ZIF-8;palladium nanoparticles;mechanochemical method;Suzuki-Miyaura coupling reaction,
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