Citation: LIU Chun-Bo, WANG Qian-Qian, BAI Hong-Ye, CHE Guang-Bo, ZHANG Qing, LI Chun-Xiang. Hydrothermal Syntheses and Properties of Compounds Based on1,10-Phenanthroline- 5,6-dione and Keggin-Type Polyoxometalate[J]. Chinese Journal of Inorganic Chemistry, ;2014, (2): 391-397. doi: 10.11862/CJIC.2014.039
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Three compounds based on Keggin-type polyoxometalate (POMs) using1,10-phen-5,6-dione (Do) as neutral organic ligand, namely, (HDo)6(PW12O40)2·H2O (1), [Cu(Do)2(H2O)]2[Cu(Do)2(PW12O40)(H2O)](PW12O40)(2) and [Pb(Do)2(PW12O40)](HDo)(3), have been synthesized under hydrothermal conditions and characterized by elemental analyses, infrared spectra, inductively coupled plasma analyses, X-ray photoelectron spectroscopy and single-crystal X-ray diffraction. Compounds 1 and 2 are zero-dimensional structures, and compound 3 exhibits one-dimensional chain. The thermal stabilities and photoluminescent properties of three compounds have also been investigated. CCDC: 767622, 1; 767623, 2; 767619, 2.
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