Citation: HUANG Qing-Li, ZHU Xia-Shi. Synthesis and Characterization of SERS-Active Silver Nanomaterial[J]. Chinese Journal of Inorganic Chemistry, ;2014, (2): 442-450. doi: 10.11862/CJIC.2014.019 shu

Synthesis and Characterization of SERS-Active Silver Nanomaterial

HUANG Qing-Li ,
ZHU Xia-Shi ^,

1.
College of Chemistry & Chemical Engineering, Yangzhou University, Yangzhou, Jiangsu 225009, China

Corresponding author: ZHU Xia-Shi,
Received Date: 8 July 2013
Available Online: 12 September 2013
Fund Project:

Three-dimensional (3D) hierarchical silver nanomaterials (HSNs) were prepared by a simple surfactant-free wet-chemical method at room temperature. The as-prepared HSNs exhibit spherical morphologies and are constructed with many 2Dnanoflakes as building blocks. Field emission scanning electron microscopy (FESEM) studies show that diammonium 2-(carboxymethyl)-2-hydroxysuccinate (diammonium hydrogen citrate) (C₆H₁₄N₂O₇) plays a key role in the formation of such HSNs. X-ray diffraction (XRD) and transmission electron microscopy (TEM) results confirm the formation of HSNs. The optical properties and surface-enhanced Raman scattering (SERS) effect were also investigated by UV-Vis and Raman spectra. The HSNs could be served as highly sensitive surface-enhanced Raman scattering (SERS) substrates for chemical detection.
- wet-chemical method;silver;surface-enhanced Raman scattering (SERS);Rhodamine (R6G and RB)
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